我(Wo)公(Gong)司(Si)自(Zi)主(Zhu)研(Yan)制(Zhi)的(De)QIMO-G系(Xi)列(Lie)光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)仪(Yi),(?)满(Man)足(Zu)中(Zhong)国(Guo)药(Yao)典(Dian),(?)专(Zhuan)业(Ye)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)检(Jian)测(Ce) 不(Bu)需(Xu)要(Yao)任(Ren)何(He)化(Hua)学(Xue)试(Shi)剂(Ji)
QIMO-G光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)法(Fa)简(Jian)介(Jie):(?)
由(You)于(Yu)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su) B1和(He) G1 本(Ben)来(Lai)具(Ju)有(You)较(Jiao)强(Qiang)的(De)荧(Ying)光(Guang)性(Xing),(?)但(Dan)接(Jie)触(Chu)水(Shui)以(Yi)后(Hou),(?)发(Fa)生(Sheng)荧(Ying)光(Guang)的(De)淬(Cui)灭(Mie)现(Xian)象(Xiang),(?)荧(Ying)光(Guang)性(Xing)基(Ji)本(Ben)消(Xiao)失(Shi),(?)很(Hen)难(Nan)用(Yong)液(Ye)相(Xiang)色(Se)谱(Pu)检(Jian)测(Ce)出(Chu)来(Lai),(?)所(Suo)以(Yi)我(Wo)们(Men)可(Ke)以(Yi)采(Cai)用(Yong)衍(Yan)生(Sheng)的(De)方(Fang)法(Fa)使(Shi)黄(Huang)曲(Qu)霉(Mei) B1 和(He) G1 的(De)荧(Ying)光(Guang)性(Xing)增(Zeng)强(Qiang)。(?)目(Mu)前(Qian)衍(Yan)生(Sheng)的(De)方(Fang)法(Fa)主(Zhu)要(Yao)有(You)三(San)氟(Fu)乙(Yi)酸(Suan)衍(Yan)生(Sheng)法(Fa),(?)碘(Dian)衍(Yan)生(Sheng)法(Fa)等(Deng)。(?)三(San)氟(Fu)乙(Yi)酸(Suan)衍(Yan)生(Sheng)法(Fa),(?)操(Cao)作(Zuo)步(Bu)骤(Zhou)繁(Fan)琐(Suo),(?)试(Shi)验(Yan)重(Zhong)复(Fu)性(Xing)很(Hen)差(Cha),(?)而(?)且(Qie)三(San)氟(Fu)乙(Yi)酸(Suan)毒(Du)性(Xing)很(Hen)强(Qiang);(?)碘(Dian)衍(Yan)生(Sheng)法(Fa),(?)需(Xu)要(Yao)柱(Zhu)后(Hou)衍(Yan)生(Sheng)泵(Beng),(?)还(Huan)要(Yao)配(Pei)制(Zhi)碘(Dian)衍(Yan)生(Sheng)液(Ye),(?)操(Cao)作(Zuo)也(Ye)很(Hen)繁(Fan)琐(Suo)。(?)而(?)本(Ben)光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)器(Qi)不(Bu)需(Xu)要(Yao)任(Ren)何(He)化(Hua)学(Xue)试(Shi)剂(Ji),(?)直(Zhi)接(Jie)连(Lian)接(Jie)于(Yu)色(Se)谱(Pu)柱(Zhu)与(Yu)荧(Ying)光(Guang)检(Jian)测(Ce)器(Qi)之(Zhi)间(Jian),(?)操(Cao)作(Zuo)简(Jian)单(Dan),(?)检(Jian)测(Ce)结(Jie)果(Guo)准(Zhun)确(Que),(?)灵(Ling)敏(Min)度(Du)高(Gao)。(?)
QIMO-G光(Guang)化(Hua)学(Xue)柱(Zhu)后(Hou)衍(Yan)生(Sheng)器(Qi)具(Ju)有(You)以(Yi)下(Xia)特(Te)点(Dian):(?)
1.无(Wu)需(Xu)使(Shi)用(Yong)化(Hua)学(Xue)物(Wu)质(Zhi)((?)省(Sheng)钱(Qian)的(De)同(Tong)时(Shi),(?)也(Ye)避(Bi)免(Mian)操(Cao)作(Zuo)人(Ren)员(Yuan)接(Jie)触(Chu)有(You)毒(Du)化(Hua)学(Xue)物(Wu)质(Zhi))(?);(?)
2.增(Zeng)加(Jia)HPLC仪(Yi)器(Qi)的(De)寿(Shou)命(Ming)((?)没(Mei)有(You)腐(Fu)蚀(Shi)性(Xing)酸(Suan)流(Liu)经(Jing)毛(Mao)细(Xi)管(Guan))(?);(?)
3.无(Wu)需(Xu)冲(Chong)洗(Xi)步(Bu)骤(Zhou);(?)
4.结(Jie)果(Guo)与(Yu)电(Dian)化(Hua)学(Xue)方(Fang)法(Fa)((?)溴(Xiu)衍(Yan)生(Sheng))(?)一(Yi)致(Zhi)。(?)
5.黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)B1、(?)B2、(?)G1、(?)G2的(De)最(Zui)低(Di)检(Jian)测(Ce)限(Xian)均(Jun)小(Xiao)于(Yu)0.5 PPB。(?)
6.符(Fu)合(He)AOAC 2005.08,(?)AOAC2008.02,(?)AOAC Aa 11-05,(?)中(Zhong)国(Guo)台(Tai)湾(Wan)标(Biao)准(Zhun)((?)食(Shi)字(Zi)0981800370号(Hao)公(Gong)告(Gao))(?)和(He)欧(Ou)盟(Meng)药(Yao)典(Dian)2.8.18标(Biao)准(Zhun)分(Fen)析(Xi)方(Fang)法(Fa)。(?)
7.符(Fu)合(He)中(Zhong)国(Guo)国(Guo)家(Jia)标(Biao)准(Zhun)和(He)进(Jin)出(Chu)口(Kou)检(Jian)验(Yan)标(Biao)准(Zhun)
8.使(Shi)用(Yong)光(Guang)化(Hua)学(Xue)柱(Zhu)后(Hou)衍(Yan)生(Sheng)器(Qi)可(Ke)在(Zai)线(Xian)实(Shi)现(Xian)对(Dui)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)B1、(?)G1进(Jin)行(Xing)衍(Yan)生(Sheng),(?)不(Bu)需(Xu)要(Yao)任(Ren)何(He)化(Hua)学(Xue)试(Shi)剂(Ji)。(?) 光(Guang)化(Hua)学(Xue)在(Zai)线(Xian)衍(Yan)生(Sheng)系(Xi)统(Tong),(?)不(Bu)仅(Jin)帮(Bang)助(Zhu)您(Nin)获(Huo)得(De)重(Zhong)复(Fu)性(Xing)好(Hao)的(De)结(Jie)果(Guo),(?)还(Huan)可(Ke)以(Yi)帮(Bang)助(Zhu)您(Nin)降(Jiang)低(Di)化(Hua)学(Xue)物(Wu)质(Zhi)的(De)污(Wu)染(Ran)和(He)危(Wei)害(Hai)。(?)
要(Yao)准(Zhun)确(Que)测(Ce)定(Ding)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)含(Han)量(Liang),(?)需(Xu)将(Jiang)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)B1和(He)G1衍(Yan)生(Sheng),(?)提(Ti)高(Gao)其(Qi)荧(Ying)光(Guang)强(Qiang)度(Du)。(?)这(Zhe)种(Zhong)用(Yong)于(Yu)液(Ye)相(Xiang)-(?)荧(Ying)光(Guang)法(Fa)测(Ce)定(Ding)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)时(Shi)进(Jin)行(Xing)柱(Zhu)后(Hou)光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)的(De)装(Zhuang)置(Zhi)。(?)((?)又(You)叫(Jiao)柱(Zhu)后(Hou)衍(Yan)生(Sheng)装(Zhuang)置(Zhi), 光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)装(Zhuang)置(Zhi),(?)光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)器(Qi))(?)。(?)光(Guang)化(Hua)学(Xue)柱(Zhu)后(Hou)衍(Yan)生(Sheng)器(Qi)可(Ke)以(Yi)在(Zai)254nm下(Xia)用(Yong)光(Guang)化(Hua)学(Xue)的(De)方(Fang)法(Fa)对(Dui)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)B1和(He)G1进(Jin)行(Xing)衍(Yan)生(Sheng),(?)与(Yu)电(Dian)化(Hua)学(Xue)溴(Xiu)衍(Yan)生(Sheng)方(Fang)法(Fa)是(Shi)等(Deng)同(Tong)的(De)。(?)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)B2和(He)G2不(Bu)受(Shou)该(Gai)衍(Yan)生(Sheng)步(Bu)骤(Zhou)的(De)影(Ying)响(Xiang)。(?)
光(Guang)化(Hua)学(Xue)柱(Zhu)后(Hou)衍(Yan)生(Sheng)器(Qi)包(Bao)括(Kuo)下(Xia)列(Lie)组(Zu)件(Jian):(?)
带(Dai)有(You)开(Kai)关(Guan)的(De)灯(Deng)架(Jia)(Lamp holder with switch)
紫(Zi)外(Wai)灯(Deng),(?)254nm(U.V. lamp,254nm)
反(Fan)应(Ying)池(Chi)架(Jia)(Reactor holder)
特(Te)殊(Shu)设(She)计(Ji)的(De)编(Bian)织(Zhi)的(De)反(Fan)应(Ying)线(Xian)圈(Quan)((?)knitted reactor coils)(?)
Peek连(Lian)接(Jie)管(Guan)两(Liang)根(Gen)
Peek接(Jie)头(Tou)4个(Ge)
Peek两(Liang)通(Tong)一(Yi)个(Ge)
安(An)装(Zhuang)与(Yu)使(Shi)用(Yong)
将(Jiang)衍(Yan)生(Sheng)器(Qi) ,(?)一(Yi)端(Duan)连(Lian)接(Jie)色(Se)谱(Pu)柱(Zhu),(?)一(Yi)段(Duan)连(Lian)接(Jie)检(Jian)测(Ce)器(Qi),(?)无(Wu)连(Lian)接(Jie)方(Fang)向(Xiang)要(Yao)求(Qiu)。(?)
适(Shi)用(Yong)范(Fan)围(Wei)
该(Gai)光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)器(Qi)广(Guang)泛(Fan)应(Ying)用(Yong)于(Yu)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)和(He)磺(Huang)胺(An)类(Lei)药(Yao)物(Wu)的(De)HPLC法(Fa)检(Jian)测(Ce),(?)它(Ta)能(Neng)够(Gou)增(Zeng)强(Qiang)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)B1和(He)G1的(De)荧(Ying)光(Guang)强(Qiang)度(Du),(?)黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)B1和(He)G1检(Jian)测(Ce)限(Xian)能(Neng)够(Gou)达(Da)到(Dao)0.1ppb;(?)还(Huan)能(Neng)够(Gou)增(Zeng)强(Qiang)磺(Huang)胺(An)类(Lei)药(Yao)物(Wu)的(De)荧(Ying)光(Guang)强(Qiang)度(Du):(?)磺(Huang)胺(An)嘧(Mi)啶(Ding)((?)Sulfadiazine)(?),(?)磺(Huang)胺(An)吡(Bi)啶(Ding)((?)Sulfapyridine)(?),(?)磺(Huang)胺(An)甲(Jia)基(Ji)嘧(Mi)啶(Ding)((?)Sulfamerazine)(?),(?)磺(Huang)胺(An)二(?)甲(Jia)嘧(Mi)啶(Ding)((?)Sulfamethazine)(?),(?)磺(Huang)胺(An)对(Dui)甲(Jia)氧(Yang)嘧(Mi)啶(Ding)((?)Sulfamethoxydiazine)(?),(?)磺(Huang)胺(An)喹(Kui)啉(Lin)((?)Sulfaquinoxaline)(?),(?)检(Jian)测(Ce)限(Xian)达(Da)到(Dao)10ppb左(Zuo)右(You)。(?)
光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)器(Qi)使(Shi)用(Yong)时(Shi)置(Zhi)于(Yu)HPLC柱(Zhu)和(He)检(Jian)测(Ce)器(Qi)之(Zhi)间(Jian),(?)进(Jin)行(Xing)柱(Zhu)后(Hou)连(Lian)续(Xu)光(Guang)化(Hua)学(Xue)衍(Yan)生(Sheng)反(Fan)应(Ying)提(Ti)高(Gao)荧(Ying)光(Guang)、(?)紫(Zi)外(Wai)、(?)电(Dian)化(Hua)学(Xue)检(Jian)测(Ce)和(He)化(Hua)学(Xue)发(Fa)光(Guang)检(Jian)测(Ce)器(Qi)的(De)灵(Ling)敏(Min)度(Du)和(He)/或(Huo)响(Xiang)应(Ying)的(De)选(Xuan)择(Ze)性(Xing)。(?)
部(Bu)分(Fen)客(Ke)户(Hu):(?)
陕(Shan)西(Xi)阔(Kuo)成(Cheng)检(Jian)测(Ce),(?)青(Qing)海(Hai)央(Yang)宗(Zong)药(Yao)业(Ye),(?)甘(Gan)肃(Su)金(Jin)昌(Chang)市(Shi)药(Yao)品(Pin)检(Jian)验(Yan)所(Suo),(?)宁(Ning)夏(Xia)北(Bei)方(Fang)民(Min)族(Zu)大(Da)学(Xue),(?)赤(Chi)峰(Feng)粮(Liang)油(You)检(Jian)测(Ce),(?)四(Si)川(Chuan)双(Shuang)信(Xin)科(Ke)技(Ji),(?)山(Shan)东(Dong)青(Qing)华(Hua)农(Nong)牧(Mu)发(Fa)展(Zhan)公(Gong)司(Si),(?)安(An)徽(Hui)东(Dong)盛(Sheng)友(You)邦(Bang)制(Zhi)药(Yao),(?)徐(Xu)州(Zhou)医(Yi)药(Yao)集(Ji)团(Tuan),(?)浙(Zhe)江(Jiang)农(Nong)业(Ye)大(Da)学(Xue),(?)青(Qing)海(Hai)畜(Xu)牧(Mu)兽(Shou)医(Yi)科(Ke)学(Xue)院(Yuan),(?)广(Guang)西(Xi)玉(Yu)林(Lin)质(Zhi)检(Jian)所(Suo),(?)武(Wu)汉(Han)大(Da)学(Xue)等(Deng)((?)经(Jing)销(Xiao)商(Shang)客(Ke)户(Hu)未(Wei)列(Lie))(?)
黄(Huang)曲(Qu)霉(Mei)毒(Du)素(Su)G1、(?)B1、(?)G2、(?)B2浓(Nong)度(Du)依(Yi)次(Ci)为(Wei)10μ(?)g/L、(?)10μ(?)g/L、(?)2.5μ(?)g/L、(?)2.5μ(?)g/L。(?)